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Die Strukturabhängigkeit der Festkörperfluoreszenz bei Phosphanylanthracenen

The relationship of solid-state fluorescence and molecular structure in phosphanylanthracenes

by Gerald Harald Schwab
Doctoral thesis
Date of Examination:2008-04-30
Date of issue:2008-05-30
Advisor:Prof. Dr. Dietmar Stalke
Referee:Prof. Dr. Dietmar Stalke
Referee:Prof. Dr. Dr. h.c. Herbert W. Roesky
crossref-logoPersistent Address: http://dx.doi.org/10.53846/goediss-2224

 

 

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Abstract

English

Four major aims have been pursued in the course of this thesis: 1. Synthesis and charactarization of 9-bromo-10-phosphanylanthracenes. 2. Investigation of the relationship between crystal structure and fluorescence properties of host/guest-complexes of 9,10-bis(diphenylthiophosphoryl)anthracene [(Ph2P=S)2(C14H8)]. 3. Lithiation-reactions of 9-Bromo-10-phosphanylanthracenes and subsequent treatment with chlorophosphanes. 4. Syntheses of phosphanyl-substituted anthracene derivatives, which exhibit additional nitrogen atoms as potential donors in metal-complexes.
Keywords: Anthracene; phosphorus; fluorescence; host/guest-systems; X-ray diffraction

Other Languages

Im Rahmen dieser Dissertation wurden im Wesentlichen vier Ziele verfolgt: 1. Synthese und Charakterisierung von 9-Brom-10-phosphanylanthracenen. 2. Untersuchung des Zusammenhangs zwischen Kristallstruktur und Fluoreszenzverhalten von Wirt/Gast-Komplexen von 9,10-Bis(diphenylthiophosphoryl)anthracen [(Ph2P=S)2(C14H8)]. 3. Möglichkeiten zur Lithiierung von 9-Brom-10-phosphanylanthracenen und nachfolgende Umsetzung mit Chlorphosphanen. 4. Darstellung von phosphanylsubstituierten Anthracenderivaten, die außerdem über Stickstoffatome als potentielle Donoren für Metall-Komplexe verfügen.
Schlagwörter: Anthracen; Phosphor; Fluoreszenz; Wirt/Gast-Systeme; Röntgenstrukturanalyse
 

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